Since I'll be bringing up a bunch of starting material in the next few weeks this is the first of many ridiculously large reactions. There is the possibility of explosion in this one (mostly right at the begining) hence the blast "wrangler" (really called the blast shield but it would mostly focus/wrangle the blast). I just left it up cause well its safer and has more of a bad ass effect in the hood. The actual reaction is just adding Sodium Azide to N-Acetylsulfonyl chloride.
Tuesday, January 30, 2007
Blast Wrangler
Since I'll be bringing up a bunch of starting material in the next few weeks this is the first of many ridiculously large reactions. There is the possibility of explosion in this one (mostly right at the begining) hence the blast "wrangler" (really called the blast shield but it would mostly focus/wrangle the blast). I just left it up cause well its safer and has more of a bad ass effect in the hood. The actual reaction is just adding Sodium Azide to N-Acetylsulfonyl chloride.
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